纺织学报 ›› 2020, Vol. 41 ›› Issue (12): 73-80.doi: 10.13475/j.fzxb.20200402708

• 纺织工程 • 上一篇    下一篇

三维机织角联锁SiCf/SiC复合材料弯曲性能及损伤机制

杨甜甜1, 王岭2, 邱海鹏2, 王晓猛2, 张典堂1(), 钱坤1   

  1. 1.生态纺织教育部重点实验室(江南大学), 江苏 无锡 214122
    2.航空工业复合材料技术中心, 北京 101300
  • 收稿日期:2020-04-10 修回日期:2020-07-08 出版日期:2020-12-15 发布日期:2020-12-23
  • 通讯作者: 张典堂
  • 作者简介:杨甜甜(1996—),女,硕士生。主要研究方向为陶瓷基复合材料。
  • 基金资助:
    国家自然科学基金项目(11702115);军委科技委基础强化项目(2017-JCJQ-ZD-035);国家科技重大专项资助项目(2017-VI-0007-0076);江苏省自然科学基金项目(BK20170166)

Bending property and damage mechanism of three-dimensional woven angle interlock SiCf/SiC composites

YANG Tiantian1, WANG Ling2, QIU Haipeng2, WANG Xiaomeng2, ZHANG Diantang1(), QIAN Kun1   

  1. 1. Key Laboratory of Eco-Textiles(Jiangnan University), Ministry of Education, Wuxi, Jiangsu 214122, China
    2. Aerospace Composites Technology Center, Beijing 101300, China
  • Received:2020-04-10 Revised:2020-07-08 Online:2020-12-15 Published:2020-12-23
  • Contact: ZHANG Diantang

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摘要：

为解决陶瓷基复合材料在服役环境中由于弯曲而导致失效的问题,从理论上分析了经向和纬向弯曲过程中复合材料弯曲受力与内部纤维之间的相互作用机制。以SiCf/SiC复合材料为例,利用微计算机断层扫描技术获得其内部纤维结构和孔隙等三维图像;并在此基础上,分别对三维机织角联锁SiCf/SiC复合材料经向和纬向进行弯曲性能测试,从细观、微观尺度分析弯曲损伤机制。结果表明:三维机织角联锁SiCf/SiC复合材料的纬向和经向性能明显不同,且纬向试样的弯曲强度大于经向试样;SiCf/SiC复合材料的弯曲损伤模式复杂,经向试样裂纹主要沿着经纱与纬纱接触点扩展,而纬向试样裂纹主要在纬纱束之间产生,并最终导致弯曲破坏。

关键词: 三维机织角联锁织物, SiCf/SiC复合材料, 先驱体浸渍裂解, 三点弯曲试验, 损伤机制

Abstract:

Targeting at the bending failure of ceramic matrix composites in service environment, the interaction mechanism between the bending stress of the composite material and the internal fibers during warp and weft bending was theoretically analyzed. Taking SiCf/SiC composite materials as an example, three-dimensional (3-D) images of internal fiber structure and pores were obtained using micro computed tomography. On this basis, the warp and weft directions of the three-dimensional woven angle interlock SiCf/SiC composite were tested respectively, and the bending damage mechanism was analyzed in the meso and micro scales. The results show that weft and warp performance of SiCf/SiC composite are significantly different, and the bending strength of the weft specimen is larger than that of the warp specimen. The bending damage modes of 3-D woven angle interlock SiCf/SiC composites are complex, in which the warp cracks mainly propagate at the warp and weft contact points, while the cracks of weft specimen mainly occur between the weft bundles, eventually leading to bending failure.

Key words: three-dimensional woven angle interlock fabric, SiCf/SiC composite, polymer Infiltration and pyrolysis, three-point bending test, damage mechanism

中图分类号: 

  • TB332

图1

三维机织角联锁SiC纤维预制件形态"

图2

三维机织角联锁SiCf/SiC复合材料形貌"

图3

三维机织角联锁 SiCf/SiC复合材料试样件"

图4

三维机织角联锁 SiCf/SiC复合材料三点弯曲试验"

图5

三维机织角联锁SiCf/SiC复合材料经向和纬向弯曲强度-挠度曲线"

表1

三维机织角联锁 SiCf/SiC复合材料弯曲力学性能"

试样
名称		 弯曲强
度/MPa		 弯曲模
量/GPa		 平均弯曲
强度/MPa		 平均弯曲
模量/GPa
经向-1 327.57 52.17 299.33 51.52
经向-2 268.79 48.74
经向-3 301.63 48.65
纬向-1 367.12 47.65 394.56 45.87
纬向-2 401.74 42.15
纬向-3 414.82 47.81
标准偏差 346.95±52.52 47.86±2.96

图6

SiCf/SiC复合材料经向和纬向弯曲受力图"

图7

经向SiCf/SiC复合材料损伤破坏超景深扫描图"

图8

纬向SiCf/SiC复合材料损伤破坏超景深扫描图"

图9

不同放大倍数下经向SiCf/SiC复合材料断面损伤电镜照片"

图10

不同放大倍数下纬向SiCf/SiC复合材料断面损伤电镜照片"

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