纺织学报 ›› 2008, Vol. 29 ›› Issue (6): 1-6.

• 纤维材料 •    下一篇

纳米ATO在制备抗静电PET单体EG中的分散性

陈晓蕾1.2;王鲁民1.2   

  1. 1.中国水产科学研究院东海水产研究所 上海200090;2.中国水产科学研究院农业部海洋与河口渔业重点开放实验室;上海200090
  • 收稿日期:2007-04-26 修回日期:2007-11-14 出版日期:2008-06-15 发布日期:2008-06-15

Dispersibility of nano-ATO in EG for preparing antistatic PET

CHEN Xiaolei;WANG Lumin;   

  1. 1.East China Sea Fisheries Research Institute;Chinese Academy of Fishery Sciences;Shanghai 200090;China;2.Key and Open Laboratory of Marine and Estuarine Fisheries;Ministry of Agriculture;Chinese Academy of Fishery Sciences;Shanghai 200090;China
  • Received:2007-04-26 Revised:2007-11-14 Online:2008-06-15 Published:2008-06-15

摘要: 以乙二醇(EG)为分散介质,研究分散方法、分散剂种类、分散剂浓度、分散液pH值和球磨时间等工艺条件对纳米锑掺杂二氧化锡(ATO)在EG中分散性的影响。用TEM和分散液的吸光度对各工艺条件下的分散情况进行表征。研究结果表明:采用球磨分散方法,选择硅烷偶联剂KH570为分散剂,分散剂对ATO的质量分数为1.5%,分散液pH值为8.5,球磨时间为36 h的工艺条件,ATO在EG中的分散效果最佳,为制备分散性能优良的纳米复合抗静电纤维提供了前提条件。

Abstract: EG was used as dispersion medium,the effects of dispersion methods,dispersion time,kinds and concentrations of dispersants,pH of the suspension and ball-milling time on the dispersibility of nano-ATO in EG for preparing antistatic PET were studied.TEM and absorbency of the suspension were used to characterize the dispersibility under different process conditions.The results show: when ball-milling is adopted as dispersing method and KH570 is used as dispersant,the time of ball-milling is 36 h,concentration of the dispersant is 1.5% and pH of the suspension is 8.5,the addition of nano-ATO in EG produces best dispersion results,which provides a precondition for preparing antistatic nanocomposites with good dispersion.

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