茜草植物染料染色莫代尔纤维的超声波处理

doi:10.13475/j.fzxb.20171103207

纺织学报 ›› 2019, Vol. 40 ›› Issue (04): 83-89.doi: 10.13475/j.fzxb.20171103207

茜草植物染料染色莫代尔纤维的超声波处理

李洋¹^,², 张元明², 姜伟¹^,², 张建明³, 王思社³, 苏建军³, 韩光亭¹^,²^,³()

1.青岛大学纺织服装学院, 山东青岛 266071
2.省部共建生物多糖纤维成形与生态纺织国家重点实验室(青岛大学), 山东青岛 266071
3.山东省恒丰植物染工业化生产技术研究院, 山东德州 253000

收稿日期:2017-11-16 修回日期:2018-12-17 出版日期:2019-04-15 发布日期:2019-04-16
通讯作者: 韩光亭
作者简介:李洋(1992—),男,硕士生。主要研究方向为功能纺织品开发与设计。
基金资助:
山东省重点研发计划项目(2016ZDJS08A04)

Ultrasonic treatment of Modal fiber dyed with madder

LI Yang¹^,², ZHANG Yuanming², JIANG Wei¹^,², ZHANG Jianming³, WANG Sishe³, SU Jianjun³, HAN Guangting¹^,²^,³()

1. College of Textiles & Clothing, Qingdao University, Qingdao, Shandong 266071, China
2. State Key Laboratory of Bio-Fibers and Eco-Textiles(Qingdao University), Qingdao, Shandong 266071, China
3. Shandong Hengfeng Plant Dyeing Industrialization Production Technology Research Institute, Dezhou, Shandong 253000, China

Received:2017-11-16 Revised:2018-12-17 Online:2019-04-15 Published:2019-04-16
Contact: HAN Guangting

摘要/Abstract

摘要：

为改善茜草植物染料染色莫代尔纤维的可纺性,采用超声波处理方法去除染色后纤维表面附着颗粒物,通过试验探讨超声波功率密度、温度、时间对颗粒物去除的影响。在此基础上选取试验因素和水平,用Box-Behnken试验设计方法,研究各变量及其交互作用对茜草植物染料染色纤维表面颗粒附着物去除的影响。结果表明:超声波处理温度对纤维表面颗粒物的去除影响最大,功率密度影响最小;利用Design Expert软件得到回归方程的预测模型对工业化处理有预测作用;超声波去除纤维表面颗粒物的最佳条件为超声波功率密度 0.67 W/cm²,超声波处理温度43 ℃,超声波处理时间22 min。

关键词: 植物染料, 莫代尔纤维, 超声波处理, Box-Behnken试验, 茜草, 染色

Abstract:

In order to improve the spinnability of the Modal fiber dyed with madder, ultrasonic treatment was employed to remove the attached particulate matters on the surface of the dyed fibers. The influence of ultrasonic power density, temperature and time on the removal of particulate matters was discussed by single factor test. The experimental factors and levels were selected on the basis of the single factor experiment. The effects of the variates and their interactions on the removal of attached particulate matters on the dyed fiber surface were then studied by the Box-Behnken experiment. The results show that ultrasonic temperature has the greatest effect on the removal of particulate matters on the surface of the fiber, and the influence of power density is the least. The prediction model of regression equation obtained by using Design Expert software has a predictive effect on industrialization. The optimum conditions for the ultrasonic particle removal are as follows: ultrasonic power density of 0.67 W/cm², ultrasonic temperature of 43 ℃ and ultrasonic time of 22 min.

Key words: plant dyeing, Modal fiber, ultrasonic treatment, Box-Behnken test, madder, dyeing

中图分类号:

TS102.2

李洋, 张元明, 姜伟, 张建明, 王思社, 苏建军, 韩光亭. 茜草植物染料染色莫代尔纤维的超声波处理[J]. 纺织学报, 2019, 40(04): 83-89.

LI Yang, ZHANG Yuanming, JIANG Wei, ZHANG Jianming, WANG Sishe, SU Jianjun, HAN Guangting. Ultrasonic treatment of Modal fiber dyed with madder[J]. Journal of Textile Research, 2019, 40(04): 83-89.

图/表 15

图1

图2

图3

图4

图5

图6

图7

表1

表2

表3

回归方程方差分析"

方差来源	平方和/10^-4	自由度	均方/10^-3	F值	p值	显著性
模型	400.00	9	4.434	18.600	0.000 4	^***
x₁	0.17	1	0.017	0.071	0.797 6
x₂	2.04	1	0.204	0.850	0.386 2
x₃	3.49	1	0.349	1.470	0.265 3
x₁x₂	1.35	1	0.135	0.570	0.475 6
x₁x₃	33.15	1	3.315	13.910	0.007 4	^***
x₂x₃	10.99	1	1.099	4.160	0.068 9
$x 1 2$	76.21	1	7.621	31.980	0.000 8	^***
$x 2 2$	150.00	1	15.000	61.950	0.000 1	^***
$x 3 2$	88.36	1	8.836	37.080	0.000 5	^***
残差	16.68	7	0.238
失拟相	11.94	3	0.398	3.360	0.136 3
净误差	4.74	4	0.119
总离差	420.00	16

表3

图8

图9

图10

图11

图12

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水平	因素
水平	功率密度/ (W·cm^-2)	超声波处理时间/min	超声波处理温度/℃
-1	0.30	15.0	30
0	0.65	22.5	45
1	1.00	30.0	60

序号	编码值			颗粒物质量浓度/(g·L^-1)
序号	A	B	C	颗粒物质量浓度/(g·L^-1)
1	-1	-1	0	0.114 953
2	1	-1	0	0.152 400
3	-1	1	0	0.124 315
4	1	1	0	0.138 491
5	-1	0	-1	0.132 072
6	1	0	-1	0.169 652
7	-1	0	1	0.179 816
8	1	0	1	0.102 248
9	0	-1	-1	0.163 099
10	0	1	-1	0.112 047
11	0	-1	1	0.113 348
12	0	1	1	0.128 595
13	0	0	0	0.236 254
14	0	0	0	0.222 746
15	0	0	0	0.237 725
16	0	0	0	0.249 761
17	0	0	0	0.225 02

茜草植物染料染色莫代尔纤维的超声波处理

Ultrasonic treatment of Modal fiber dyed with madder

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