纺织品卷烟味去除效果的评价方法

doi:10.13475/j.fzxb.20190103006

纺织学报 ›› 2020, Vol. 41 ›› Issue (02): 77-82.doi: 10.13475/j.fzxb.20190103006

纺织品卷烟味去除效果的评价方法

于昕辰¹^,²^,³^,⁴, 陈红¹^,³^,⁴, 方艳萍⁵, 丁雪梅¹^,³^,⁴()

1.东华大学服装与艺术设计学院, 上海 200051
2.西安工程大学服装与艺术设计学院, 陕西西安 710048
3.上海国际设计创新研究院, 上海 200080
4.东华大学现代服装设计与技术教育部重点实验室, 上海 200051
5.青岛海尔股份有限公司, 山东青岛 266101

收稿日期:2019-01-14 修回日期:2019-11-17 出版日期:2020-02-15 发布日期:2020-02-21
通讯作者: 丁雪梅
作者简介:于昕辰(1989—),女,博士生。主要研究方向为纺织服装产品护理技术与理论。
基金资助:
国家重点研发计划资助项目(2018YFF0215703);中央高校基本科研业务费专项资金资助项目(2232019G-08);上海市科委技术标准专项项目(17DZ2202900);上海市设计学IV类高峰学科资助项目(DD18005)

Research on assessment of removing effectiveness of cigarette odor from textiles

YU Xinchen¹^,²^,³^,⁴, CHEN Hong¹^,³^,⁴, FANG Yanping⁵, DING Xuemei¹^,³^,⁴()

1. College of Fashion and Design, Donghua University, Shanghai 200051, China
2. School of Apparel and Art Design, Xi'an Polytechnic University, Xi'an, Shaanxi 710048, China
3. Shanghai International Institute of Design & Innovation, Shanghai 200080, China
4. Key Laboratory of Clothing Design & Technology, Ministry of Education, Donghua University, Shanghai 200051, China
5. Haier Co., Ltd., Qingdao, Shandong 266101, China

Received:2019-01-14 Revised:2019-11-17 Online:2020-02-15 Published:2020-02-21
Contact: DING Xuemei

摘要/Abstract

摘要：

为评价家用滚筒烘干机去除纺织品吸附卷烟味的效果,更好地指导家电企业对纺织品护理产品的开发和优化,基于干衣机烘干去除卷烟味的方法及特点,建立了主观评价法和客观评价法相结合的除烟臭效果检测方法。主观评价法采用嗅觉判定6级强度法,通过研究消费者对卷烟味的可接受程度,得到除味效果的合格标准为1级及以下。客观评价法采用顶空固相微萃取/气相色谱法测定烟气特征物质(烟碱、苯酚及4-吡咯烷基吡啶)浓度的变化,同时建立了异味成分减少率作为评价指标。研究结果表明,主客观评价均可表征异味浓度的差异,且结果具有一致性,主客观相结合的方法可有效应用于清洁法去除纺织品吸附卷烟味消臭效果的评价。

关键词: 纺织品, 卷烟味, 除烟臭, 顶空固相微萃取法, 气相色谱

Abstract:

In order to evaluate the effectiveness of domestic tumble drying on removing the cigarette odor from textiles and enable the development and optimization of textile care products that can refresh textiles, based on the principles and characteristics of laundering methods, an evaluation method on deodorization with the combination of subjective and objective assessment was established. The 6-level intensity method was used for subjective evaluation. The acceptability for cigarette odor was no more than 1 grade. As for the objective evaluation, headspace solid phase micro-extraction and gas chromatography-mass spectrometry was used for testing the concentration of typical substances (L-nicotine, phenol, 4-pyrrolidinopyridine) of cigarette odor. In the meantime, deodorization rate was put forward to indicate the reduction of typical substances. According to the results of case study, both of subjective and objective evaluation method can be utilized to demonstrate the difference of odor concentration, and evaluation results of both methods turned out to be consistent. Therefore, the method with the combination of subjective and objective assessment can be effectively applied for evaluating the performance of laundering method on removing cigarette odor form textiles.

Key words: textiles, cigarette odor, deodorization, headspace solid phase microextraction, gas chromatograph

中图分类号:

TS973.1

于昕辰, 陈红, 方艳萍, 丁雪梅. 纺织品卷烟味去除效果的评价方法[J]. 纺织学报, 2020, 41(02): 77-82.

YU Xinchen, CHEN Hong, FANG Yanping, DING Xuemei. Research on assessment of removing effectiveness of cigarette odor from textiles[J]. Journal of Textile Research, 2020, 41(02): 77-82.

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等级	描述
0	无异味
1	较难感知到的异味(检测浓度界限值)
2	仅可分辨出较弱的异味(分辨浓度界限值)
3	很容易感知到的异味
4	较强异味
5	强烈异味

测试者编号	2级样品
测试者编号	评级结果/级	是否接受	评级结果/级	是否接受
1	2	×	1	√
2	2	×	1	√
3	2	×	1	√
4	2	√	1	√
5	2	×	1	√
6	2	×	1	√
7	2	√	0.5	√
8	2	×	1	√
9	2	×	0.5	√
10	2	×	1	√

中文名称	英文名称	CAS号	分子式
烟碱 (尼古丁)	L-nicotine	54-11-5	C₁₀H₁₄N₂
苯酚	phenol	108-95-2	C₆H₆O
4-吡咯烷基吡啶	4-pyrrolidinopyridine	2456-81-7	C₉H₁₂N₂

测试程序编号	负载量/ kg	喷蒸汽量/ min	滚筒电动机转速/ (r·min^-1)	加热丝功率/ W	风速/ (m·s^-1)	烘干时间/ min
1	1	0	1 100	0	6.8	20
2	1	10	1 100	0	6.8	20
3	1	10	1 100	2 000	6.8	20
4	3块分别附着异味样块的负载布	放置于环境温湿度为(20±2)℃、(65±2)%的室内20 min,房间内置空气循环系统

程序	样块香烟味臭气等级
初始异味样块	5
吹冷风程序	3
喷蒸汽+吹冷风	2
喷蒸汽+加热烘干	0
自然晾晒	4

纺织品卷烟味去除效果的评价方法

Research on assessment of removing effectiveness of cigarette odor from textiles

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异味特征物质	初始异味样品	吹冷风程序样品		喷蒸汽+吹冷风样品		喷蒸汽+加热烘干样品		自然晾晒样品
异味特征物质	色谱峰面积	色谱峰面积	r/%	色谱峰面积	r/%	色谱峰面积	r/%	色谱峰面积	r/%
烟碱	3 304 102	202 662	94	8 9307	97	0	100	582 306	82
苯酚	1 306 364	0	100	0	100	0	100	122 608	91
4-吡咯烷基吡啶	154 320	8 781	94	5 546	96	0	100	30 324	80

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