纺织学报 ›› 2010, Vol. 31 ›› Issue (3): 68-71.

• 纺织工程 • 上一篇    下一篇

大麻纤维针刺毡Mg(OH)2整理后的热性能分析

杜兆芳;刘晓华;程贤生;宋雷   

  1. 安徽农业大学轻纺工程与艺术学院
  • 收稿日期:2008-12-22 修回日期:2009-04-30 出版日期:2010-03-15 发布日期:2010-03-15
  • 通讯作者: 杜兆芳

Analysis on thermal properties of the hemp needle-punched felt treated by Mg(OH)2

DU Zhaofang;LIU Xiaohua; CHENG Xiansheng; SONG Lei   

  1. College of Light–Textile Engineering and Art, Anhui Agricultural University
  • Received:2008-12-22 Revised:2009-04-30 Online:2010-03-15 Published:2010-03-15
  • Contact: DU Zhaofang

摘要:

采用Mg(OH)2阻燃剂,在阻燃剂质量浓度300g/L,黏合剂体积分数为20%,浸渍时间20min的工艺条件下对大麻纤维针刺毡进行阻燃整理,用热重分析(TG)法和差热分析(DTA)法对Mg(OH)2阻燃整理前后大麻纤维针刺毡热性能进行对比分析。结果表明:经Mg(OH)2阻燃整理后的大麻纤维针刺毡初始热解阶段为0 ~330℃、主要热解阶段在330~400℃、残渣热解阶段在400~600℃;且热失重和最大热失重速率明显降低、剩炭率增加、热解起始温度升高;第1个放热峰值降低了50%、无第2个放热峰出现,说明阻燃剂Mg(OH)2对大麻纤维针刺毡有较好的阻燃效果。

Abstract:

The flame-retardant finishing of the hemp needle-performed with Mg(OH)2 (mass concentration 300g/L) and adhesive (volume concentration 20%) with imprenating time 20 min. The thermal properties the hemp needle-punched felt before and after flame retardant finishing were analyzed by using thermo gravimetry (TG) and differential thermal analysis (DTA). The results revealed that the hemp needle-punched felt treated by Mg(OH)2 has the initial pyrolysis stage 0 ~ 330 ℃, the main pyrolysis stage 330 ~ 400 ℃, and the residual pyrolysis stage 400 ~ 600 ℃. The speed of hot weightlessness and maximum hot weightlose reduces obviously, and the rate of remains of the carbon increases and the initial temperature of thermal decomposition increases. The first exothermic peak value reduced 50% , no second exothermic peak is observed, indicating that the Mg(OH)2 has imparted good flame-retardant effect to the hemp needle-punched felt.

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