纺织学报 ›› 2015, Vol. 36 ›› Issue (12): 69-74.

• 染整与化学品 • 上一篇    下一篇

亚临界萃取羊毛脂工艺的响应面法优化

  

  • 收稿日期:2014-12-30 修回日期:2015-09-10 出版日期:2015-12-15 发布日期:2015-12-10

Extracting of lanolin from raw wool with optimized subcritical fluid technology by response surface methodology

  • Received:2014-12-30 Revised:2015-09-10 Online:2015-12-15 Published:2015-12-10

摘要:

为提高羊毛脂的回收率,以原为原料从中提取羊毛脂,研究了亚临界萃取羊毛脂过程中不同的萃取条件下的提取率。分别考察了亚临界溶剂选择、萃取温度、萃取时间、萃取次数及料溶比等因素对羊毛脂萃取率的影响,并在单因素实验基础上利用响应面法进行优化,得出萃取率最高的工艺条件为:温度65℃、时间10min、料溶比1:10、萃取5次,萃取率可以达到6.03%;考虑到实际生产效益及对纤维性状影响,最终得到亚临界萃取羊毛脂的最佳工艺为:温度50℃,次数3次,萃取率4.43%

Abstract:

In order to improve the recovery rate of lanolin, raw wool was studied as raw material for the extraction of lanolin, and extraction yield of lanolin under different conditions by the subcritical extraction process was also investigated. The influence on lanolin extracting rate by extraction condition including the subcritical solvent, extraction temperature, time, times and liquid-solid ratio were examined, respectively, and on the basis of single factor experiment, the response surface methodology was used to optimization the technological parameter. It is concluded that technology conditions with the highest extraction rate is at 65 ℃, extracting 10 min, with the ratio 1:10 of solid to liquid, and repeat the whole extraction process for 5 times, and on this condition, extraction rate of lanolin can reach 6.03%. Considering the actual production efficiency and influence on fiber properties, the resulting optimum process for subcritical extraction lanolin is at 50 ℃, 3 times, and extraction rate is 4.43%.

中图分类号: 

  • TS133
No related articles found!
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed   
[1] 郭兴峰;王瑞;黄故;房昕. 接结经纱对三维正交机织物结构的影响[J]. 纺织学报, 2005, 26(1): 56 -58 .
[2] 姜铸;郭伟. 我国新型工业化进程中纺织产业升级的途径[J]. 纺织学报, 2008, 29(7): 117 -121 .
[3] 饶崛;徐卫林. 热状态下UHMWPE纤维的力学性能[J]. 纺织学报, 2009, 30(01): 5 -8 .
[4] 王羽;陈志强;马维新;王照民. A272D型并条机改装压力捧牵伸的研究[J]. 纺织学报, 1994, 15(05): 25 -27 .
[5] 储才元;闵夏莲;孙爱萍. 热熔粉剂的粘结性能及其对非织造布性能影响的探讨[J]. 纺织学报, 1994, 15(07): 15 -18 .
[6] 刘恩华;李树锋;程博闻;杜启云. 聚丙烯腈基中空碳纤维膜制备及结构研究[J]. 纺织学报, 2006, 27(4): 19 -21 .
[7] 王连贵. 多功能花式捻线机罗拉支承结构讨论[J]. 纺织学报, 1984, 5(09): 33 -35 .
[8] 胡杰. 粗细纱支在同一织物中的应用[J]. 纺织学报, 1986, 7(05): 32 -33 .
[9] 曹亚春;柳德康;徐福华;戴琦兴;许逊;陈如荣. 一种改进的试样复摇车[J]. 纺织学报, 1986, 7(05): 45 -46 .
[10] 宁俊;陈桂玲;李淑珍;陆亚新. 北京服装产业发展对策[J]. 纺织学报, 2006, 27(6): 107 -110 .