JOURNAL OF TEXTILE RESEARCH ›› 2018, Vol. 39 ›› Issue (01): 1-5.doi: 10.13475/j.fzxb.20170603605

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Preparation and properties of wet-spinning graphene fibers

  

  • Received:2017-06-13 Revised:2017-11-10 Online:2018-01-15 Published:2018-01-16

Abstract:

In order to better realize the application of graphene fibers in function textile area, the graphene oxides fiber were prepared by wet-spinning method using graphene oxides solution as spinning dope and calcium chloride solution with different content as coagulation bath. The graphene fibers were obtained by chemical reduction of the as-prepared graphene oxides fibers in the aqueous solution of hydroiodic acid. The oxidation degree and structure morphology of graphene oxides were characterized by X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy (TEM), which indicated that the carbon and oxygen atom value of graphene oxides was 1:1, and graphene oxides showed thin and crumpled morphology. The influence of tensile strength was researched by CaCl2 coagulation bath with different mass fraction. The graphene fibers derived from 20% CaCl2 coagulation bath, exhibited high electrical conductivity of 180 S/ cm and good tensile strength of 892 MPa.

Key words: graphene fibers, wet-spinning, coagulation bath, conductivity, tensile strength

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