Journal of Textile Research ›› 2019, Vol. 40 ›› Issue (8): 64-68.doi: 10.13475/j.fzxb.20180902505

• Textile Engineering • Previous Articles     Next Articles

Establishment and application of fabrics attenuated total reflection Fourier transform infrared spectroscopy spectrum library

WEI Zihan, LI Wenxia(), DU Yujun, MA Jingwen, ZHENG Jiahui   

  1. School of Materials Science and Engineering, Beijing Institute of Fashion Technology, Beijing 100029, China
  • Received:2018-09-11 Revised:2019-05-15 Online:2019-08-15 Published:2019-08-16
  • Contact: LI Wenxia E-mail:liwenxia307@163.com

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Abstract: Aim

ing at many processes, long time-consuming and polluting the environment when identifying pure textile fabrics by conventional methods and predicting the component contented of blended fabrics, the attenuated total reflection Fourier transform infrared spectroscopy(ATR-IR) spectra of various pure spun and two-component blended fabrics were tested by using Fourier transform infrared spectrometer in combination with the attenuated total reflection (ATR) attachment, and the ATR-IR spectral library was established, which was composed of 205 pure and blended fabric samples of back-to-face as well as warp and weft with identical components. The samples comprising polyester/cotton, polyester/wool, polyester/polyamide, silk/cotton and polyester/viscose blended fabric were selected from 753 samples. 20 samples of unknown fabrics were identified and predicted by using the searching function of the self-built spectrum library, and the accuracy of recognition can reach 100% for pure spun. For blended fabric, the quantitative predicted results were not significantly different from those of national standard method by the T-test analysis in less than 3% error. The prediction greatly facilitates the rapid detection and quantification of samples.

Key words: attenuated total reflection, Fourier transform infrared spectroscopy, nondestructive testing, identification of fabric component

CLC Number: 

  • S941.45

Fig.1

ATR-IR spectra of indigo and indigo dyed denim"

Fig.2

ATR-IR spectra of polyester fabrics with different colors"

Fig.3

ATR-IR spectra of polyester/cotton fabric front and back"

Fig.4

ATR-IR spectra of pure wool fabrics with different textures"

Fig.5

ATR-IR spectra of coated fabrics"

Fig.6

ATR-IR spectra of core-spun yarn fabrics"

Tab.1

Retrieval results of unknown fabric samples from ATR-IR spectral library"

样品
编号		 组
成		 国标法
测定值/%		 谱库预
测值/%		 匹配
度/%		 绝对
误差/
%		 相对
误差/
%
1 T 100.00 100.00 98.01 0.00 0.00
2 PAN 100.00 100.00 98.96 0.00 0.00
3 T/C 40.90/59.10 40.50/59.50 96.32 0.40 1.00
4 Md 100.00 100.00 99.17 0.00 0.00
5 Tel 100.00 100.00 98.92 0.00 0.00
6 C 100.00 100.00 99.73 0.00 0.00
7 T/C 63.10/36.90 64.90/35.10 97.27 1.80 2.90
8 T/C 81.80/18.20 79.60/20.40 98.97 1.20 1.50
9 CA 100.00 100.00 98.92 0.00 0.00
10 T/W 31.50/68.50 32.20/67.80 99.39 0.70 2.20
11 S/C 62.00/38.00 62.50/37.50 93.47 0.50 0.80
12 T/W 70.00/30.00 70.10/29.90 98.99 0.10 0.10
13 PP 100.00 100.00 98.77 0.00 0.00
14 Ram 100.00 100.00 98.46 0.00 0.00
15 T/W 56.70/43.30 56.90/43.10 98.07 0.20 1.90
16 T/W 48.30/51.70 49.60/50.40 98.32 1.30 2.70
17 T/N 77.50/22.50 79.00/21.00 98.97 1.50 1.90
18 PE 100.00 100.00 99.83 0.00 0.00
19 T/N 83.30/16.70 83.20/16.80 98.46 0.10 0.10
20 T/R 66.70/33.30 68.80/31.20 99.93 2.10 3.20

Tab.2

True and predicted values of blended fabrics for T-test analysis%"

样品编号 待测织物类别 待测组分 真实值 预测值
3 T/W T 31.50 32.20
7 T/W T 56.70 56.90
8 T/C T 40.90 40.50
10 T/W T 70.10 70.90
11 T/C T 81.80 79.60
12 T/R T 66.70 68.80
15 T/C T 63.10 64.90
16 T/W T 48.30 49.60
20 S/C S 62.00 62.50
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