Journal of Textile Research ›› 2020, Vol. 41 ›› Issue (02): 77-82.doi: 10.13475/j.fzxb.20190103006

• Dyeing and Finishing & Chemicals • Previous Articles     Next Articles

Research on assessment of removing effectiveness of cigarette odor from textiles

YU Xinchen1,2,3,4, CHEN Hong1,3,4, FANG Yanping5, DING Xuemei1,3,4()   

  1. 1. College of Fashion and Design, Donghua University, Shanghai 200051, China
    2. School of Apparel and Art Design, Xi'an Polytechnic University, Xi'an, Shaanxi 710048, China
    3. Shanghai International Institute of Design & Innovation, Shanghai 200080, China
    4. Key Laboratory of Clothing Design & Technology, Ministry of Education, Donghua University, Shanghai 200051, China
    5. Haier Co., Ltd., Qingdao, Shandong 266101, China
  • Received:2019-01-14 Revised:2019-11-17 Online:2020-02-15 Published:2020-02-21
  • Contact: DING Xuemei E-mail:fddingxm@dhu.edu.cn

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Abstract:

In order to evaluate the effectiveness of domestic tumble drying on removing the cigarette odor from textiles and enable the development and optimization of textile care products that can refresh textiles, based on the principles and characteristics of laundering methods, an evaluation method on deodorization with the combination of subjective and objective assessment was established. The 6-level intensity method was used for subjective evaluation. The acceptability for cigarette odor was no more than 1 grade. As for the objective evaluation, headspace solid phase micro-extraction and gas chromatography-mass spectrometry was used for testing the concentration of typical substances (L-nicotine, phenol, 4-pyrrolidinopyridine) of cigarette odor. In the meantime, deodorization rate was put forward to indicate the reduction of typical substances. According to the results of case study, both of subjective and objective evaluation method can be utilized to demonstrate the difference of odor concentration, and evaluation results of both methods turned out to be consistent. Therefore, the method with the combination of subjective and objective assessment can be effectively applied for evaluating the performance of laundering method on removing cigarette odor form textiles.

Key words: textiles, cigarette odor, deodorization, headspace solid phase microextraction, gas chromatograph

CLC Number: 

  • TS973.1

Tab.1

Level of odor strength"

等级 描述
0 无异味
1 较难感知到的异味(检测浓度界限值)
2 仅可分辨出较弱的异味(分辨浓度界限值)
3 很容易感知到的异味
4 较强异味
5 强烈异味

Tab.2

Assessment of acceptance for cigarette odor"

测试者
编号		 2级样品 1级样品
评级结果/级 是否接受 评级结果/级 是否接受
1 2 × 1 √
2 2 × 1 √
3 2 × 1 √
4 2 √ 1 √
5 2 × 1 √
6 2 × 1 √
7 2 √ 0.5 √
8 2 × 1 √
9 2 × 0.5 √
10 2 × 1 √

Tab.3

Typical substances of smoke"

中文名称 英文名称 CAS号 分子式
烟碱
(尼古丁)		 L-nicotine 54-11-5 C10H14N2
苯酚 phenol 108-95-2 C6H6O
4-吡咯烷基吡啶 4-pyrrolidinopyridine 2456-81-7 C9H12N2

Tab.4

Details of drying programs"

测试
程序
编号		 负载量/
kg		 喷蒸
汽量/
min		 滚筒电动
机转速/
(r·min-1)		 加热丝
功率/
W		 风速/
(m·s-1)		 烘干
时间/
min
1 1 0 1 100 0 6.8 20
2 1 10 1 100 0 6.8 20
3 1 10 1 100 2 000 6.8 20
4 3块分别附着异味样块的负载布 放置于环境温湿度为(20±2)℃、(65±2)%的室内20 min,房间内置空气循环系统

Tab.5

Results of subjective assessment of deodorization"

程序 样块香烟味臭气等级
初始异味样块 5
吹冷风程序 3
喷蒸汽+吹冷风 2
喷蒸汽+加热烘干 0
自然晾晒 4

Tab.6

Results of objective assessment of deodorization"

异味特
征物质		 初始异味样品 吹冷风程序样品 喷蒸汽+吹冷风样品 喷蒸汽+加热烘干样品 自然晾晒样品
色谱峰面积 色谱峰面积 r/% 色谱峰面积 r/% 色谱峰面积 r/% 色谱峰面积 r/%
烟碱 3 304 102 202 662 94 8 9307 97 0 100 582 306 82
苯酚 1 306 364 0 100 0 100 0 100 122 608 91
4-吡咯烷
基吡啶		 154 320 8 781 94 5 546 96 0 100 30 324 80
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