Journal of Textile Research ›› 2021, Vol. 42 ›› Issue (04): 55-61.doi: 10.13475/j.fzxb.20200800207

• Fiber Materials • Previous Articles     Next Articles

Polyvinyl alcohol as reinforcement in damping composites consisting of chlorinated polyethylene and hindered phenol

JIANG Sheng1,2(), JI Limei1,2   

  1. 1. Division of Science and Technology, Jiangsu College of Engineering and Technology, Nantong, Jiangsu 226001, China
    2. Jiangsu Advanced Textile Engineering Technology Center, Nantong, Jiangsu 226001, China
  • Received:2020-08-03 Revised:2021-01-05 Online:2021-04-15 Published:2021-04-20

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Abstract:

A series of damping composites consisting of polyvinyl alcohol (PVA) acted as reinforcement and the mixture of chlorinated polyethylene (CPE) and 4,4'-methylene-bis-(2,6-dis-tert-butylph-enol) (AO 4426) acting as the matrix were prepared in order to broaden the application field of PVA. The properties and microstructure of the composites were measured and characterized by means of dynamic thermomechanical analyzer, differential thermal analyzer, Fourier infrared spectrometer, scanning electron microscope and mechanical test equipment. The results show that the composites still maintains characteristics of two damping peaks of CPE-AO 4426 composite after adding PVA,and the storage modulus and area under loss modulus curve at the damping temperature range of composites increased with the increase of PVA mass fraction, indicating that the damping performance of composites obtained greater improvement. The hydrogen bonds were formed between hydroxyl group of PVA and hydroxyl group of AO 4426. The fracture stress and the strain of the composite both demonstrate an increase and then a decrease with increase of PVA.

Key words: polyvinyl alcohol, chlorinated polyethylene, 4,4'-methylene-bis-(2,6-di-tert-butylphenol), microcrystalline enrichment, damping property, damping composite

CLC Number: 

  • TQ327.11

Fig.1

Schematic diagram of size mixing device"

Tab.1

Preparation formula of PVA/(CPE-AO 4426) membranes"

试样编号 PVA质量分数/% CPE-AO 4426质量分数/%
1# 0 100
2# 10 90
3# 20 80
4# 30 70
5# 40 60

Fig.2

Effect of mass fraction of PVA on storage modulus of PVA/(CPE-AO 4426) composites"

Fig.3

Effect of mass fraction of PVA on loss factor of PVA/(CPE-AO 4426) composites"

Fig.4

SEM images of PVA/(CPE-AO 4426) composites with different mass fraction of PVA (×3 000)"

Fig.5

Effect of mass fraction of PVA on LA values of PVA/(CPE-AO 4426) composites"

Fig.6

FT-IR spectra of AO 4426 and PVA/(CPE-AO 4426) composites (a) and its partial waveband (b)"

Fig.7

DSC curves of AO 4426 and PVA/(CPE-AO 4426) composites"

Fig.8

Sress-strain curves of PVA/(CPE-AO 4426) composites with different mass fraction of PVA"

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