Journal of Textile Research ›› 2023, Vol. 44 ›› Issue (03): 126-131.doi: 10.13475/j.fzxb.20210504006

• Dyeing and Finishing & Chemicals • Previous Articles     Next Articles

Wear performances of cotton fabrics reactive-dyed in salt-free waste cooking oil-water system

QI Haotong, ZHANG Linsen, HOU Xiuliang, XU Helan()   

  1. College of Textile Science and Engineering, Jiangnan University, Wuxi, Jiangsu 214122, China
  • Received:2021-05-17 Revised:2022-12-22 Online:2023-03-15 Published:2023-04-14

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Abstract:

Objective Conventional aqueous phase dyeing produces a large amount of wastewater containing high concentrations of dyes and salts. A new waste cooking oil-water two-phase dyeing system was investigated to prove the effectiveness in cotton dyeing, and the minimal discharge of hydrolyzed dyes, salts and alkali.

Method An oil-water two-phase dyeing system and a conventional aqueous dyeing system were adopted to dye cotton fabrics. Wear performances include capillary adsorption, combustion behavior, kubbing resistance, wrinkle-recovery behavior, water vapor permeability, moisture regain, and hand feeling of fabrics dyed in the two systems were studied and compared.

Results Wicking heights of two-phase dyed cotton fabric are about 10% and 20% lower than their water dyed counterparts in both warp and weft directions, respectively. A small amount of oil may remain in the fiber interior, causing plug of the capillaries. Continuous burning time of two-phase dyed cotton fabric are slightly shorter than that of aqueous dyed cotton fabric. Smoldering time of two-phase dyed cotton fabrics were (8.14 ± 0.58)s and (7.90±1.43) s, respectively, and that of aqueous dyed cotton fabric were (7.70 ± 0.67) s and (8.24 ± 0.61) s, respectively. The limit oxygen index (LOI) of two-phase dyed cotton fabric was (17.60±0.05)%, close to (17.85±0.06)%, the LOI value of aqueous dyed counterparts. With regard to wear resistance, two-phase dyed cotton fabric resembled aqueous dyed cotton fabric with 24±2 and 25±2 cycles, respectively. The warp and weft elastic recovery angles of two-phase dyed cotton fabric are (68.32 ± 10.98)(°) and (65.80 ± 8.31)(°), respectively, higher than the angles of aqueous dyed cotton fabric are (57.92 ± 9.97)(°) and (54.92 ± 11.78)(°), respectively. Recovery angles of two-phase dyed cotton fabric are (62.14 ± 7.23)(°) and (54.10 ± 8.80)(°), respectively, also moderately higher than that of aqueous dyed cotton fabric. Moisture regain of two-phase dyed and aqueous dyed cotton fabrics are (8.75±0.84)% and (9.59±0.23)%, respectively, while moisture transmittance of two-phase dyed and aqueous dyed cotton fabrics are (3 827±453) and (2 562 ± 136) g/(m2·24 h), respectively. Overall hand feeling indices of two-phase dyed and aqueous dyed cotton fabrics are 0.60±0.02 and 0.58±0.02, respectively, indicating similar hand feeling of the two fabrics.

Conclusion In general, although there were some slight differences in wear performances and hand feeling between cotton fabrics dyed in a two-phase system and an aqueous system, most of the properties could meet the industry standards.

Key words: waste cooking oil, cotton fabric, reactive dye, dyeing, low-alkali, fabric hand feeling, wear performance

CLC Number: 

  • TS197

Fig.1

Process curve of conventional aqueous dyeing"

Fig.2

Oil water two phase dyeing process curve"

Fig.3

Process flow chart of oil-water two phase dyeing"

Tab.1

Performance test results of dyed cotton fabric"

染色方式 芯吸高度/cm 续燃时间/s 阴燃时间/s 极限氧指数/%
经向 纬向 经向 纬向 经向 纬向
油水两相染色 8.6±0.4 6.5±0.5 2.60±0.60 2.92±0.58 8.14±0.58 7.90±1.43 17.60±0.05
水相染色 9.5±0.6 7.9±0.6 4.64±0.37 5.30±0.94 7.70±0.67 8.24±0.61 17.85±0.06
染色方式 磨破次数 急弹回复角/(°) 缓弹回复角/(°) 透湿率/
(g·(m2·24 h)-1)		 回潮率/%
经向 纬向 经向 纬向
油水两相染色 24±2 62.14±7.23 54.10±8.80 68.32±10.98 65.80±8.31 3 827±453 8.75±0.84
水相染色 25±2 45.36±11.45 45.68±13.56 57.92±9.97 54.92±11.78 2 562±136 9.59±0.23

Fig.4

Morphologies of cotton fabric after burning. (a) Traditional water-phase dyed cotton fabric; (b) Cotton fabric dyed with oil-water two-phase system"

Tab.2

Results of fabric hand test"

染色
方式		 平均弯曲刚度/
(cN·mm·rad-1)		 弯曲功/
(cN·mm·rad)		 压缩功/
(cN·mm)		 压缩回弹率/
%		 平均压缩刚度/
(cN·cm-2·mm-1)		 平均回弹刚度/
(cN·cm-2·mm-1)		 表面粗糙度振幅/
μm
油水两
相染色		 137.60±53.32 298.45±54.94 647.25±68.24 30.50±3.54 538.35±16.48 3 787.35±331.20 15.65±0.49
水相
染色		 117.00±43.57 348.47±122.68 673.20±26.10 39.00±6.24 613.40±170.93 3 953.07±225.29 14.50±1.25
染色
方式		 热导率/(W·(m·℃)-1) 最大热流量/
(W·m-2)		 表面摩
擦因数		 光滑度 柔软度 温暖感 总指数
压缩 回复
油水两
相染色		 23.10±0.14 23.30±0.14 1 197.00±44.41 0.30±0.01 0.52±0.02 0.57±0.04 0.70±0.06 0.60±0.02
水相
染色		 23.93±0.57 24.07±0.35 1 252.23±20.00 0.27±0.01 0.56±0.06 0.61±0.08 0.45±0.14 0.58±0.02
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