Journal of Textile Research ›› 2022, Vol. 43 ›› Issue (07): 81-89.doi: 10.13475/j.fzxb.20210810509

• Textile Engineering • Previous Articles     Next Articles

Structural and laminar damage mechanisms in layer-to-layer orthogonal angle-interlock woven fabrics and composites

JIA Xuefei1, ZHUANG Yi2, TANG Yujing1(), LI Shanshan3, SHI Wen4, ZHANG Lei3, LIU Ming5, ZHOU Jiangming5   

  1. 1. SINOPEC (Beijing) Research Institute of Chemical Industry, Co., Ltd., Beijing 100013, China
    2. China Petroleum & Chemical Corporation, Beijing 100728, China
    3. State Key Laboratory of Biological Fiber Manufacturing Technology, China Textile Academy Co., Ltd., Beijing 100025, China
    4. Carle Zeiss (Shanghai) Co., Ltd., Shanghai 200131, China
    5. SINOPEC Baling Petrochemical Co., Ltd., Yueyang, Hunan 414014, China
  • Received:2021-08-30 Revised:2022-03-24 Online:2022-07-15 Published:2022-07-29
  • Contact: TANG Yujing E-mail:tangyj.bjhy@sinopec.com

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Abstract:

In order to analyze the internal structure and the load bearing of layer-to-layer orthogonal angle-interlock woven fabrics and composites, X-ray computed tomography (Micro CT) volume pixels was used to extract non-destructively the internal structure. The micro-structure of layer-to-layer orthogonal angle-interlock the woven fabric was observed by three-dimensional reconstruction, and the twisting and extrusion of monofilaments inside the fabric was observed. The distribution of pores and high-density impurities in the composite were reconstructed and the quantitative estimations were carried out. The results show that the composite demonstrated good integrity after the laminar damage test, there are phenomena shch as pore deformation, delarmination, fiber bending and lamella fractures inside. It was confirmed that the unique structure of the layer-to-layer orthogonal angle-interlock woven fabric effectively improved the interlaminar mechanical properties of the composites, highlighting the importance of non-destructive X-ray computed tomography in analyzing the imaging data of fiber reinforced composites.

Key words: layer-to-layer orthogonal angle-interlock, composites, woven structure, defects, micro computed tomography, interlaminar shear

CLC Number: 

  • TB332

Fig.1

Schematic diagram of stucture of woven fabric"

Tab.1

Parameter settings"

试样名称 物镜倍数 体素/μm 视场范围/mm 投影张数
机织物 4 5.0 Φ5.0×5.0 2 001
4 2.0 Φ2.0×2.0 2 501
4 0.7 Φ0.7×0.7 3 201
机织复合材料 0.4 30.0 Φ30.0×30.0 1 001
4 4.0 Φ4.0×4.0 2 001
20 0.5 Φ0.5×0.5 3 501

Fig.2

3-D image and 2-D section view of woven fabric at 5.0 μm. (a) Side view; (b) 2-D rendering of specimens at z direction; (c) Top view of three-dimensional rendering; (d)2-D rendering of specimens at y direction"

Fig.3

Internal morphology of woven fabric at 0.7 μm volume pixels. (a) Fiber bundle; (b) Interface of fiber bundles"

Fig.4

3-D segmentation renderings (a), 2-D virtual slices (b) and defect distribution maps (c) of woven fabric composite at different volume pixels"

Fig.5

Defect distribution of woven fabric composite at 4.0 μm volume pixels. (a) Reconstructed 3-D morphologies of high density particles; (b) Distribution of high density particles in fabric; (c) Distribution of high density particles in matrix; (d) 3-D image of porosity defect; (e) Distribution of porosity defect in fabric; (f) Distribution of porosity defect in matrix"

Fig.6

Load-displacement curves of woven fabric composite in fracture tests at x direction"

Fig.7

Woven fabric composite after fracture test"

Fig.8

2-D rendering of specimens of woven fabric composite after fracture test. (a) x direction; (b) y direction; (c) z direction"

Fig.9

Damage mechanism of woven fabric composite. (a) Matrix stability under loading; (b) Extrusion-bending; (c) Matrix cracking; (d) Fracture and crack growth"

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