JOURNAL OF TEXTILE RESEARCH ›› 2014, Vol. 35 ›› Issue (5): 87-0.

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Survey analysis of triclosan in textiles by liquid chromatography - tandem mass spectrometry

  

  • Received:2013-04-27 Revised:2014-01-03 Online:2014-05-15 Published:2014-05-09
  • Contact: Chun-Mei E-mail:87863506@qq.com

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Abstract: The method for the determination triclosan in five major categories of textiles by liquid chromatography - tandem mass spectrometry (LC-MS/MS) was established, and 15 samples were randomly selected from the market for survey analysis. The method has good linear relationship in the range of 0.01-0.5 μ g/mL, linear equation is: y=3.5e4x-994, correlation coefficient was 0.9998, the determination of the lower limit was 0.025 mg/L, the average recovery rate was 85.6 - 107.2%, the relative standard deviation was less than 7%. Only 2 samples was detected in all samples, showed that in textiles had been add triclosan.

Key words: liquid chromatography-tandem mass spectrometry, triclosan, textiles, survey

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