JOURNAL OF TEXTILE RESEARCH ›› 2015, Vol. 36 ›› Issue (05): 59-62.

Previous Articles     Next Articles

Preparation of wool keratin solution with Ionic liquid

  

  • Received:2014-04-01 Revised:2014-08-11 Online:2015-05-15 Published:2015-05-12
  • Contact: 姚金波 YAO Jin-Bo E-mail:yao-yaojinbo@tjpu.edu.cn

Abstract:

The dissolution of wool fiber was studied in the solvent system with 1 - allyl - 3 - methyl imidazole chloride (Amim [Cl]) as main solvent and mercaptoethanol as auxiliary reagent. The orthogonal experiments result indicates that the optimal dissolving process of wool fabric was that m (wool):m ( AMIM [Cl] ) :m (mercaptoethanol)= 1:8.5:1, temperature at 120 ℃ and time for 7.5 h. Under these treatment conditions, wool fibers can be completoly dissolved. The polarity of AMIM [CI] and mercaptoethanol can open the hydrogen bonds and disulfide bonds, in combination with the shearing of mechanical mixing, wool fiber can be dissolved.

Key words: ionic liquid, dissolve, wool fiber, keratin

CLC Number: 

  • TQ341+.5
[1] . Preparation and characterization of silk fibroin /polyvinyl alcohol composite membrane [J]. Journal of Textile Research, 2018, 39(11): 14-19.
[2] . Preparation of wool keratin and its modification to polyester fabrics [J]. JOURNAL OF TEXTILE RESEARCH, 2018, 39(03): 92-97.
[3] . Alkali deweighing of polyester fabrics using alkyl imidazolium Gemini ionic liquid [J]. JOURNAL OF TEXTILE RESEARCH, 2018, 39(01): 79-83.
[4] . Biological enzyme synergistic catalytic system and its mechanism on wool fiber [J]. JOURNAL OF TEXTILE RESEARCH, 2018, 39(01): 71-78.
[5] . Structural characterization and applicaion of rabbit whiting [J]. JOURNAL OF TEXTILE RESEARCH, 2017, 38(12): 20-26.
[6] . Relationship between fractal structure and warmth retention properties of wool fiber assembly [J]. JOURNAL OF TEXTILE RESEARCH, 2017, 38(08): 11-15.
[7] . Sizing properties of feather keratin-graft-polyester/cotton warp yarns poly (acrylic acid-co-methyl arylate) for polyester/cotton warp yarns [J]. JOURNAL OF TEXTILE RESEARCH, 2017, 38(05): 75-79.
[8] . Solubility and spectral characteristic of feather and down in different dissolution systems [J]. JOURNAL OF TEXTILE RESEARCH, 2017, 38(04): 27-31.
[9] . Preparation of keratin/multi-walled carbon nanotubes composite fibers [J]. JOURNAL OF TEXTILE RESEARCH, 2017, 38(02): 21-25.
[10] . Influence of asymmetry imidazolium-based ionic liquids on retarding dyeing performance of acrylic fiber [J]. JOURNAL OF TEXTILE RESEARCH, 2016, 37(10): 68-72.
[11] . Preparation and characterization of plasticizing melting system consisting of cellulose diacetate and plasticizers [J]. JOURNAL OF TEXTILE RESEARCH, 2016, 37(09): 6-11.
[12] . Preparation and characterization of lauric acid cellulose ester and its film properties [J]. JOURNAL OF TEXTILE RESEARCH, 2016, 37(01): 11-15.
[13] . Influence of graft modification on sizing properties of feather keratin [J]. JOURNAL OF TEXTILE RESEARCH, 2015, 36(08): 68-73.
[14] . Preparation of wool keratin membranes prepared by ionic liquids method and reduction  C method [J]. Journal of Textile Research, 2015, 36(06): 55-59.
[15] . Composition and structure of skin dander included in cashmere [J]. Journal of Textile Research, 2015, 36(06): 24-29.
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed   
[1] . [J]. JOURNAL OF TEXTILE RESEARCH, 1993, 14(11): 33 -34 .
[2] . [J]. JOURNAL OF TEXTILE RESEARCH, 2001, 22(05): 27 -28 .
[3] . Anti-light discoloration properties of natural fiber textiles composition[J]. JOURNAL OF TEXTILE RESEARCH, 2011, 32(5): 50 -56 .
[4] LIU Yue-xin;XU Liang-hua;ZHAO Zhi-juan;ZHANG Jun. Application of sound velocimeter during the preparation of PAN-based carbon fibers[J]. JOURNAL OF TEXTILE RESEARCH, 2005, 26(4): 7 -9 .
[5] WANG Shugen;WU Ruozi. Partial physical and chemical properties of the wool regeneration protein and polyacrylonitrile copolymerization fiber[J]. JOURNAL OF TEXTILE RESEARCH, 2007, 28(12): 9 -11 .
[6] . [J]. JOURNAL OF TEXTILE RESEARCH, 2002, 23(06): 32 -33 .
[7] ZHANG Chi, ZHANG Cheng-Jun, WU Xiao-Guang. Control system data preparation of computerize flat knitting machine[J]. JOURNAL OF TEXTILE RESEARCH, 2012, 33(8): 124 -129 .
[8] . One-step in situ preparation of nano Ag-ZnO on cotton fabric for multifunctional finishing[J]. JOURNAL OF TEXTILE RESEARCH, 2014, 35(3): 92 -0 .
[9] . Quantum chemistry study on photostability of two hemicyanine fluorescent dyes[J]. JOURNAL OF TEXTILE RESEARCH, 2016, 37(06): 83 -90 .
[10] ZHOU Yi-ling . Training about computer appliance ability for stud ent majoring in garment design[J]. JOURNAL OF TEXTILE RESEARCH, 2005, 26(1): 135 -137 .